New PDF release: Compendium of Organic Synthetic Methods -Volume 7

By Michael B. Smith

ISBN-10: 0471049239

ISBN-13: 9780471049234

ISBN-10: 047135550X

ISBN-13: 9780471355502

ISBN-10: 0471355518

ISBN-13: 9780471355519

ISBN-10: 0471367524

ISBN-13: 9780471367529

ISBN-10: 0471607134

ISBN-13: 9780471607137

ISBN-10: 0471848964

ISBN-13: 9780471848967

ISBN-10: 0471867284

ISBN-13: 9780471867289

Content material: Preface. Abbreviations. Index, Monofunctional Compounds. Index, Difunctional Compounds. advent. 1 guidance of Alkynes. 2 training of Acid Derivatives. three practise of Alcohols. four arrangements of Aldehydes. five coaching of Alkyls, Methylens, and Aryls. 6 education of Amides. 7 coaching of Amines. eight guidance of Esters. nine coaching of Ethyl Epoxides and Thioethers. 10 training of Halides and Sulfonates. eleven guidance of Hydrides. 12 training of Ketones. thirteen instruction of Nitriles. 14 training of Alkenes. 15 guidance of Oxides. sixteen guidance of Difunctional Compounds. writer Index

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Extra resources for Compendium of Organic Synthetic Methods -Volume 7

Sample text

IPrzN]zMg . cyclohexane 2. H3O+ also obtained 47% of condensation products Sanchez. R; Scott, W. , 1988, 29, 139. M. , 1988, 29, 517 aliphatic ketones give no reaction; reduces only cyclic ketones W c e . ; LaVaute, T. , 1988, 29, 525. 5 3 Yo SECTK>N 4 2 A - Alcohols From Ketones OSiMezf-Bu 1. LiAlH4 , ether Ph -78OC - RT Ph I Me 43 + Ph I Me 2. 10% aq. ; Virard, C. , 7988,29, 1021. ; Matsuda, H. J. Chem. , Chem. , 7988, 882. ; Graziani, M. , 7989, 30, 2705. NaBH4 (solid state) PhJ Ph PhJ 3d Ph 63% Toda.

7987, 52, 4020. ; Achiwa. K. Chem. , 7987, 855 L[ THF , -25OC ,5h Ph $,],B-CI 2 *Ph 6 2 Yo 98% ee , S Brown. V. J. Am. Chem. ,7988, 110, 1539. 40 a COMPENDIUM OF ORGANIC SYNTHETIC METHODS VOL 7 1. ; pak. , 1988, 29, 4453. -10°CMe ,X h M e , 70h OH lMe Ph PhAMe IRh(COD)C1]2 . ; Buono. G. , 1988, 29, 3235. T. , 1988, 29, 6199. THF , -78"C, 6h 9 8 Yo 36% ee , R Brown. S. J. Org. , 1988, 53, 1231 95% SECTDN 4 2 A Alcohols From Ketones Bakers Yeast , aq. KOH H ! ; Fuiisawa. T. , 7989, 30, 381 1. 80% ee , R volne.

Prep. Proceed. , 1989, 21, 373. ; Perichon, J. , 1987, 28, 5 5 . phmph 1 . ; Chikamatsu, H. J. Chem. ,Chem. , 1987, 334. G. J. Org. , 1987, 52, 3233. ; w c X B ' [activated Zno/Me3SiCl] ether, O°C 7 9 Yo . Ph. , 1987, 28, 4551 0 IM 3 eq. TBAF , THF ,25OC nC6H13K , i M e , 12h 68% nC6H13 U l r n a n Paae. V. , 1987, 28, 4455. , 1988, 29, 89. OH Ph- Bu 6 1 Oo/ OSiiPrg P PhMe ,95OC, 18h sealed tube h d 98% iPr3SiO Bu Danheiser. P. , 1988, 29, 491 7 . 46 COMPENDIUM OF ORGANIC SYNTHETIC METHODS VOL 7 SECTION 42B 2 eq.

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Compendium of Organic Synthetic Methods -Volume 7 by Michael B. Smith


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