By K H Overton
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Extra info for A Review of the literature published between September 1970 and August 1971
Jefford and U. ),1970, 24, 385. Y. Bessiere-Chretien and B. Meklati, Bull. chim. France, 1971, 2591. C. W. Jefford, personal communication. l,l]octane ring system has also been synthesized by Joulain and Rouessac, following a similar path to that used by Hatem and Waegell; their note described a number of other unsuccessful routes. O 0 Acetylation of pinane (77) (90 '/" cis) with acetyl chloride and aluminium chloride under Friedel-Crafts conditions leads to the same mixture of l-chloro2-acetylmenthanes (27 1) as is obtained in a similar reaction using menth-1-ene (103), through which the reaction is assumed to pass.
Soc. chim. France, 1971,461. A . Gaiffe and J . Castanet, Compt. , 1971, 272, C, 96. A. Gaiffe and J . Castanet, Compt. , 1970, 271, C, 1012. J. M . Coxon, R. P. Garland, and M. P. Hartshorn, Chem. , 1970, 1709 (Chem. Abs. 1971, 74, 142 073, summarizing this work, is incorrect). 217 J. M. Coxon, R. P. Garland, and M. P. Hartshorn, Austral. J . Chem. 1970, 23, 2531. J. M. Coxon, R. P. Garland, and M. P. Hartshorn, Austral. J . , 1971, 24, 1481. 2 1 4 J. R. Salmon and D. Whittaker, J . Chem. Suc.
Hull, and E. S. Meeting, Los Angeles, March-April, 1971, Abstracts; see Amer. Perfumer and Cosmetics, 1971,86; issue 6, p . 72; P. R. Hull, Dim. Abs. , 1971, 31, B, 5477. i A&H2R CH,OMe CMO CHO N (84) Reagents: i, 200 " C ;ii, H,O-H + ; iii, FeNH,(SO,), or NH,OH. Scheme 2 There is a small group of alkaloids related to the iridane rnonoterpenes which have the general structure (86). 74 Thin-layer chromatography of V. ; ii, Na,SO,; iii, lN-H,SO,-acetone; iv, A . Scheme 3 73 74 75 B. Frank, U . Petersen, and F.
A Review of the literature published between September 1970 and August 1971 by K H Overton